home
news
about us
literature
contact us
Products Technology Download
thetametrisis-logo
_FR-Thermal
 

Description

FR-Thermal is an optical tool for the monitoring of the thickness and optical constants changes of polymer/photoresist films during controlled heating / cooling. By using the FR-Thermal and the especially developed algorithms provided, physicochemical properties such as the glass transition temperature of polymer films are evaluated for a wide film thickness range. The operation of the FR-Thermal tool is based on White Light Reflectance Spectroscopy (WLRS) and exploits the FR-Basic platform with the addition of a controlled heating/cooling unit. The tool is controlled by a specially developed Windows program (FR-Monitor), performing data acquisition, heating/cooling control, and film thickness and optical constants calculations. A material database is included and can easily be expanded by the user.

 

The entire system (hardware – software) is shipped ready for measurements: light source, spectrometer, reflection probe, heating/cooling unit, temperature controller, Windows™ software and can be easily used by anyone with basic computer skills without any deep knowledge of optics. The only additional part needed is a computer with two free USB ports running Windows XP/Vista/7 Operating System.

The film thickness and optical constants are calculated in real time while the physicochemical properties are determined after the completion of the measurements. Tight control over the heating and cooling rates allows for in depth study of the polymer film properties. The FR-Thermal is also ideal for many other thermal studies such as film thermal ablation, temperature dependent optical properties changes, Post Apply Bake, Post Exposure Bake thickness loss in lithography etc. For thickness measurements, all that is required in most cases is a smooth, reflective substrate. For optical constant measurements, a flat reflecting substrate is required. If the substrate is transparent, then its backside should be non reflective. FR-Thermal can handle layer stacks of up to four layers (environment and substrate are additional layers) and two parameters may be calculated e.g. the thicknesses of two films or the thickness and the optical constants of one film.

The FR-THERMAL tool has been successfully applied for the calculation of the thermal properties of various polymer films as well as on the evaluation of the effect of thermal treatment on the lithographic properties of several photoresist films over totally reflecting substrates (Si wafer).

 
Fig.1 FR-thermal tool schematic showing the reflection probe and the heating unit where teh sample is placed Fig.2 Temperature Glass (Tg) transition calculation for a PMMA film, using FR-Thermal tool
 
Specifications***
Applications
Thickness 5nm – 150μm*
Polymer Characterization
Wavelength range 200-1100nm*
Photopolymer Characterization
Accuracy 0.5 %
Biomedical
Precision 0.02nm
Semiconductor
Spot size 0.5mm
non Metal Films
Sample size 10 - 150mm, iregular shape
Optical Coating
Computer requirements PC with Windows XP/Vista/7 and a USB port available
Hardcoats
Power requirements 110V/230V AC  
Dimensions (WxLxH) 360mm x 400mm x 180mm**  
Weight 13.5Kgr*  
   
 
* Depends on the specification, please refer to FR-Basic page.
** In the height measurement does not icluded the cober top.
*** Specifications are subject to change without any notice.
 
©2010 Thetametrisis